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The
chart below schematically shows the interactive approach taken by CAFS
researchers to study brakes . The approach brings various expertise and
technologies to bear on a somewhat complex problem. Our research team
prides itself in its adaptation and development of technologies and
methods, including these areas:
• Mechanical Properties – Nanoindentation (modulus, stiffness, and hardness) • Thermal Properties – diffusivity, DSC, DTA, TGA, and expansion • Thermodynamics and kinetics data and theory • Topography – AFM and contact profilometry • Data Analysis and Modeling • Statistics (probability based sampling and assessment) • Structure and Chemistry via (FE)SEM, (S)TEM, EDX, XRD, Synchrotron, XRF, GC-MS, FTIR, AFM, XPS • Modified evaluation procedures; emphasis on energy dissipation rate (power)
The research equipment for each of the areas indicated in the chart above is as follows:
Mechanical Properties Characterization • Static measurements under tension, compression, flexure using Instron Multiproperty System • Dynamic measurements of elastic and bulk moduli using Grindosonic Tester.
Thermal Properties Characterization
DSC (RT up to 1500 oC, vacuum, gasses, air)
TGA (RT up to 1700 oC, vacuum, gasses, air)
Dilatometer (RT up to 1600 oC, vacuum, gasses, air)
Flash Thermal Diffusivity - RT (air) up to 2000 oC (vacuum or inert gasses)
density measurements (helium pycnometry or mineral spirits immersion)
Surface Topography Characterization • Contact Stylus Profilometer • Atomic Force Microscopy
Structure and Chemistry Characterization • White and Polarized Light Microscopy • Scanning Electron Microscopy (variable pressure) with EDX • Transmission Electron Microscopy with EDX • X-ray Diffraction, Synchrotron, Grazing Angle • FTIR, XPS, AES
Friction Properties Characterization • Pin on Disc Apparatus • Friction Assessment and Screening Test (FAST) • Subscale Aircraft Dynamometer • Full Scale Automotive Dynamometer
Let’s look at some brake materials… Brake
rotors are typically cast iron Brake pads fall into three categories:
semi-metallic (SM), non-asbestos organic (NAO), and hybrid. Here are
some images that reveal the construction of these materials.

Examining Brake Performance Brake
performance includes not only the safety issue of how the friction
coefficient changes under conditions, but also how the materials wear
under various conditions, the noise that is generated, and the impact
on the environment (particulate and noise pollution). Brake noise is
the number one consumer complaint in the brake industry and responsible
for most warranty returns.
It’s hard to correlate performance and bulk material composition or
bulk material properties or the properties of individual components. As
we seek answers, we are guided to look in detail at the friction layer
that is developed on both materials at the friction interface. This
friction layer is very different (compositionally and often
structurally) than the bulk materials.
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